Articles with "microwave synthesis" as a keyword



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Microwave synthesis and voltammetric simultaneous determination of paracetamol and caffeine using an MOF-199-based electrode

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Published in 2017 at "Journal of Materials Science"

DOI: 10.1007/s10853-017-1715-0

Abstract: AbstractIn the present paper, the microwave synthesis of MOF-199 and its application as an electrode modifier for the simultaneous voltammetric determination of paracetamol (PAR) and caffeine (CAF) were demonstrated. The obtained materials were characterised by… read more here.

Keywords: mof 199; microwave synthesis; electrode; determination paracetamol ... See more keywords
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Microwave synthesis and enhancement of thermoelectric figure of merit in half-Heusler TiNiSbxSn1-x

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Published in 2017 at "Ceramics International"

DOI: 10.1016/j.ceramint.2017.04.100

Abstract: Abstract The preparation of half-Heusler thermoelectric bulk is complex and time-consuming. In the present work, Sb doped TiNiSbxSn1−x bulks (x=0.01, 0.02, 0.03 and 0.04) were prepared via cold press forming, microwave synthesis and sintering in… read more here.

Keywords: figure merit; microwave synthesis; half heusler; thermoelectric figure ... See more keywords
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Hydrothermal microwave synthesis of SnO microspheres with excellent photocatalytic activity

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Published in 2019 at "Ceramics International"

DOI: 10.1016/j.ceramint.2018.10.204

Abstract: Abstract SnO samples were prepared from SnCl2 and NH4HCO3 by microwave–hydrothermal method. The effects of temperature on the composition, microstructure, and photocatalytic properties of SnO were studied. Results showed that samples synthesized at 50–90 °C for… read more here.

Keywords: microwave synthesis; synthesis sno; sno samples; sno microspheres ... See more keywords
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Microwave synthesis of charge-compensated dodecaborates bearing exohedral boron-phosphorus connectivities

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Published in 2017 at "Inorganica Chimica Acta"

DOI: 10.1016/j.ica.2017.12.027

Abstract: Abstract Solution pyrolysis of arylphosphonium salts of B12H122−,1, utilizing microwave heating provided charge-compensated monophosphine dodecaborate derivatives of general formula B12H11(PPhnR3-n)− (n = 1, R = Me; n = 2, R = Me, Et) in high yield. The resulting anions B12H11(PPh2Me)− (2), B12H11(PPhMe2)− (3),… read more here.

Keywords: compensated dodecaborates; charge; synthesis charge; microwave synthesis ... See more keywords
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Zeolitic imidazolate frameworks as novel precursors for microwave synthesis of carbon nanotubes

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Published in 2019 at "Journal of Alloys and Compounds"

DOI: 10.1016/j.jallcom.2018.12.123

Abstract: Abstract Till date metallocenes, especially ferrocene is the only reliable precursor for microwave synthesis of carbon nanotubes (CNT). In this manuscript we report the utility of cobalt or palladium based ZIF (Zeolitic imidazolate frameworks) as… read more here.

Keywords: zeolitic imidazolate; microwave synthesis; carbon nanotubes; synthesis carbon ... See more keywords
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Facile microwave synthesis of uniform magnetic nanoparticles with minimal sample processing

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Published in 2017 at "Journal of Magnetism and Magnetic Materials"

DOI: 10.1016/j.jmmm.2016.07.063

Abstract: Abstract We present a simple and rapid method for the synthesis of small magnetic nanoparticles (diameters in the order of 5–20 nm) and narrow size distributions (CV's of 20–40%). The magnetite nanoparticles were synthesized in green… read more here.

Keywords: facile microwave; magnetic nanoparticles; synthesis method; microwave synthesis ... See more keywords
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Smooth and rapid microwave synthesis of MIL-53(Fe) including superparamagnetic γ-Fe2O3 nanoparticles

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Published in 2017 at "Journal of Magnetism and Magnetic Materials"

DOI: 10.1016/j.jmmm.2017.08.013

Abstract: Abstract MIL-53(Fe) linked to superparamagnetic γ - Fe 2 O 3 nanoparticles was created using time-efficient microwave synthesis. Intermediates as well as the final product have been characterized by Dynamic Light Scattering (DLS), Infrared Spectroscopy… read more here.

Keywords: rapid microwave; smooth rapid; mil; synthesis mil ... See more keywords
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Microwave synthesis of mesoporous CuCo2S4 nanoparticles for supercapacitor applications

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Published in 2018 at "Materials Chemistry and Physics"

DOI: 10.1016/j.matchemphys.2018.05.026

Abstract: Abstract A simple, cost-effective, and ultrafast microwave method for preparing ternary Cu-Co sulfides (CuCo2S4) is reported for the first time. The electrochemical tests demonstrate the highest specific capacitance of 580 F g−1 at 1 A g−1, and an good… read more here.

Keywords: synthesis mesoporous; nanoparticles supercapacitor; microwave synthesis; mesoporous cuco2s4 ... See more keywords

Microwave synthesis, microstructure, and thermoelectric properties of Zr substituted ZrxTi1−xNiSn half-Heusler bulks

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Published in 2017 at "Materials Letters"

DOI: 10.1016/j.matlet.2017.05.023

Abstract: Abstract The half-Heusler thermoelectric bulks Zr x Ti 1−x NiSn (x = 0.1, 0.2, 0.3, 0.4) were rapidly prepared by microwave heating. The phase composition and microstructure were characterized by X-ray diffractometer (XRD) and scanning electron microscopy… read more here.

Keywords: synthesis microstructure; microwave synthesis; half heusler; microstructure ... See more keywords
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Microwave synthesis of zeolites and their related applications

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Published in 2021 at "Microporous and Mesoporous Materials"

DOI: 10.1016/j.micromeso.2021.111262

Abstract: Abstract Zeolites are an emerging class of crystalline, nanoporous, inorganic material with regular micropores and highly tunable functionalities. Zeolites have been proposed as ideal materials for applications in catalysis, adsorption, and biomedicine due to their… read more here.

Keywords: synthesis; microwave assisted; microwave; microwave synthesis ... See more keywords
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Ultrafast Microwave Synthesis of Ru-Doped MoP with Abundant P Vacancies as the Electrocatalyst for Hydrogen Generation in a Wide pH Range.

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Published in 2023 at "Inorganic chemistry"

DOI: 10.1021/acs.inorgchem.3c01299

Abstract: Molybdenum phosphide (MoP) has received increasing attention for the hydrogen evolution reaction (HER) due to its Pt-like electronic structure and high electrical conductivity. In this work, a flake-like Ru-doped MoP with phosphorus vacancy (Ru-MoP-PV) electrocatalyst… read more here.

Keywords: ultrafast microwave; microwave synthesis; doped mop; synthesis doped ... See more keywords