Mild and Efficient Degradation of Amine‐Cured Epoxy Resins Using Mixed Solvents
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DOI: 10.1002/app.57311
Abstract: Various recycling methods of epoxy resins were proposed, but they most involve harsh reaction conditions. Herein, it was reported on a mild and efficient method for the complete degradation of amine cured epoxy resin, and… read more here.
Keywords: mild efficient; degradation; cured epoxy; epoxy resins ... See more keywords
Mild and Efficient Synthesis of Diverse Organo‐AuI‐L Complexes in Green Solvents
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DOI: 10.1002/cssc.201903415
Abstract: Abstract An exceptionally mild and efficient method was developed for the preparation of (hetero)aryl‐AuI‐L complexes using ethanol or water as the reaction medium at room temperature and Ar‐B(triol)K boronates as the transmetalation partner. The reaction… read more here.
Keywords: efficient synthesis; reaction; aryl; mild efficient ... See more keywords
A Mild and Efficient Synthesis of Functionalized 2‐Fluorobenzamides from 1,2,3‐Benzotriazinones via Denitrogenative Fluorination Reactions under Thermal/Visible Light Conditions
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DOI: 10.1002/ejoc.202500375
Abstract: An efficient method for the synthesis of 2‐fluorobenzamides was established from 1,2,3‐benzotriazinones using tetrafluoroboric acid. The reactions proceeded under mild thermal conditions, providing a wide range of functionalized 2‐fluorobenzamides in 65‐80% yields. On the other… read more here.
Keywords: functionalized fluorobenzamides; mild efficient; visible light; synthesis functionalized ... See more keywords
Sulfated polyborate: mild, efficient and eco-friendly catalyst for the synthesis of 2,3-dihydroquinazolin-4(1H)-ones
Sign Up to like & getrecommendations! Published in 2017 at "Journal of the Iranian Chemical Society"
DOI: 10.1007/s13738-017-1109-x
Abstract: An efficient, inexpensive and recyclable sulfated polyborate catalyst was applied in a three-component, one-pot cyclocondensation of isatoic anhydride, aldehydes and ammonium acetate/amines to afford the corresponding 2,3-dihydroquinazolin-4(1H)-ones. The key advantages of the present method are… read more here.
Keywords: dihydroquinazolin ones; sulfated polyborate; polyborate mild; catalyst ... See more keywords
Mild and efficient rhodium-catalyzed deoxygenation of ketones to alkanes
Sign Up to like & getrecommendations! Published in 2019 at "New Journal of Chemistry"
DOI: 10.1039/c9nj02954k
Abstract: Chlorodicarbonylrhodium(i) dimer: a simple catalyst for the reduction of carbonyl compounds also. read more here.
Keywords: mild efficient; deoxygenation ketones; rhodium catalyzed; ketones alkanes ... See more keywords
The stable “F–SO2+” donor provides a mild and efficient approach to nitriles and amides
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DOI: 10.1039/d2ra05890a
Abstract: In this update, we developed a mild, efficient and practical method using fluorosulfuryl imidazolium salt A as an environment friendly promoter for conversion of oximes to nitriles or amides via β-elimination or Beckmann rearrangement in… read more here.
Keywords: so2 donor; nitriles amides; provides mild; mild efficient ... See more keywords
A mild and efficient oxidation of 2,3,6-Trimethylphenol to Trimethyl-1,4-benzoquinone with high-velocity air as an oxidant in a continuous-flow microreactor
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DOI: 10.1039/d4nj05103c
Abstract: 2.3.5-trimethyl-1.4-benzoquinone (TMQ) is an important intermediate in the synthesis of vitamin E, and the oxygen oxidation of 2.3.6-trimethylphenol (TMP) is commonly used to prepare TMQ in the industry. However, the... read more here.
Keywords: oxidation trimethylphenol; mild efficient; trimethyl benzoquinone;
A mild and efficient synthesis of N-aryl glycines by the rearrangement of 2-chloro-N-aryl acetamides
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DOI: 10.1039/d5ra02497h
Abstract: A mild and efficient one-pot procedure was developed for the synthesis of substituted N-aryl glycines from 2-chloro-N-aryl acetamides by intermolecular cyclization in the presence of CuCl2·2H2O and KOH under reflux condition in acetonitrile medium. The… read more here.
Keywords: aryl glycines; aryl acetamides; mild efficient; chloro aryl ... See more keywords
Mild and Efficient Vicinal Dibromination of Olefins Mediated by Aqueous Ammonium Fluoride
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DOI: 10.1055/s-0036-1588506
Abstract: A mild and efficient vicinal dibromination of olefins has been developed by using saturated aqueous ammonium fluoride solution as the promoter. Inexpensive and commercially available N -bromosuccinimide (NBS) was used as the brominating reagent. The… read more here.
Keywords: ammonium fluoride; vicinal dibromination; aqueous ammonium; dibromination olefins ... See more keywords
Mild, Efficient, and Highly Regioselective Synthesis of 2,6-Diiodobenzaldehyde Derivatives
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DOI: 10.1055/s-0040-1708004
Abstract: An efficient and versatile synthesis of 2,6-diiodobenzaldehydes via highly regioselective metal–iodine exchange (MIE) of 5-substituted 1,2,3-triiodobenzenes is reported. The nature of substituents (R) on the phenyl has a large influence on the reactivity of reaction… read more here.
Keywords: diiodobenzaldehyde derivatives; synthesis diiodobenzaldehyde; highly regioselective; mild efficient ... See more keywords
Mild and Efficient Heterogeneous Hydrogenation of Nitroarenes Facilitated by a Pyrolytically Activated Dinuclear Ni(II)-Ce(III) Diimine Complex
Sign Up to like & getrecommendations! Published in 2022 at "International Journal of Molecular Sciences"
DOI: 10.3390/ijms23158742
Abstract: We communicate the assembly of a solid, Ce-promoted Ni-based composite that was applied as catalyst for the hydrogenation of nitroarenes to afford the corresponding organic amines. The catalytically active material described herein was obtained through… read more here.
Keywords: efficient heterogeneous; heterogeneous hydrogenation; hydrogenation; hydrogenation nitroarenes ... See more keywords