A continuous flow-batch hybrid reactor for commodity chemical synthesis enabled by inline NMR and temperature monitoring
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DOI: 10.1016/j.tet.2018.05.070
Abstract: Inline, real time NMR and temperature measurements have been used to optimise the continuous flow synthesis of difluoromethyltrimethylsilane (TMSCF2H) by the reduction of the Ruppert-Prakash reagent (TMSCF3). These measurements were used to maximise the space-time-yield,… read more here.
Keywords: nmr temperature; flow batch; continuous flow; synthesis ... See more keywords