Introduction of a coiled solid-phase microextraction fiber based on a coating of animal bone waste for chromatographic analysis.
Sign Up to like & getrecommendations! Published in 2017 at "Journal of separation science"
DOI: 10.1002/jssc.201601240
Abstract: We attempt to introduce animal bone waste as a coating material with an organic-inorganic structure for the fabrication of a coiled solid-phase microextraction fiber for the first time. The coiled fiber was simply prepared with… read more here.
Keywords: microextraction fiber; waste; phase microextraction; solid phase ... See more keywords
Gold nanoparticles based solid-phase microextraction coatings for determining organochlorine pesticides in aqueous environmental samples.
Sign Up to like & getrecommendations! Published in 2017 at "Journal of separation science"
DOI: 10.1002/jssc.201700046
Abstract: The use of solid-phase microextraction coatings based on gold nanoparticles was investigated, focusing the attention on the preparation of nanoparticles with nonclassical reduction agents of HAuCl4 such as gallic acid and H2 O2 , rather… read more here.
Keywords: gold nanoparticles; phase microextraction; microextraction coatings; solid phase ... See more keywords
A novel sorbent based on carbon nanotube/amino-functionalized sol-gel for the headspace solid-phase microextraction of α-bisabolol from medicinal plant samples using experimental design.
Sign Up to like & getrecommendations! Published in 2018 at "Journal of separation science"
DOI: 10.1002/jssc.201700993
Abstract: A novel sol-gel coating on a stainless-steel fiber was developed for the first time for the headspace solid-phase microextraction and determination of α-bisabolol with gas chromatography and flame ionization detection. The parameters influencing the efficiency… read more here.
Keywords: sol gel; headspace solid; phase microextraction; solid phase ... See more keywords
Graphene-doped electrochemical copolymer coating of 2,2-bithiophene and 3-methylthiophene for the highly effective solid-phase microextraction of volatile benzene homologues.
Sign Up to like & getrecommendations! Published in 2018 at "Journal of separation science"
DOI: 10.1002/jssc.201701330
Abstract: We report the electrochemical fabrication of a poly(2,2-bithiophene-co-3-methylthiophene)-graphene composite coating and its application in the headspace solid-phase microextraction and gas chromatography determination of benzenes (i.e., bromobenzene, 4-bromotoluene, 2-nitrotoluene, 3-nitrotoluene and 1,2,4-trichlorobenzene). The coating was uniform… read more here.
Keywords: bithiophene methylthiophene; phase microextraction; solid phase;
Boronate affinity monolithic column incorporated with graphene oxide for the in-tube solid-phase microextraction of glycoproteins.
Sign Up to like & getrecommendations! Published in 2018 at "Journal of separation science"
DOI: 10.1002/jssc.201701417
Abstract: A poly(vinylphenylboronic acid-ethylene glycol dimethacrylate) monolithic material incorporated with graphene oxide was synthesized inside a poly(ether ether ketone) tube. This tube with boronate affinity monolith was coupled with a high-performance liquid chromatography system through a… read more here.
Keywords: graphene oxide; peroxidase; phase microextraction; solid phase ... See more keywords
Fiber-in-tube solid-phase microextraction of caffeine as a molecular tracer in wastewater by electrochemically deposited layered double hydroxide.
Sign Up to like & getrecommendations! Published in 2018 at "Journal of separation science"
DOI: 10.1002/jssc.201701539
Abstract: Modified stainless-steel wires with a layer of polyaniline conductive polymer were coated by electrochemical deposition with Zn/Al layered double hydroxide to make solid-phase microextraction fibers. The coating layer was also electrochemically deposited on the inner… read more here.
Keywords: layered double; phase microextraction; double hydroxide; solid phase ... See more keywords
Preparation and application of chlorpyrifos molecularly imprinted solid-phase microextraction probes for the residual determination of organophosphorous pesticides in fresh and dry foods.
Sign Up to like & getrecommendations! Published in 2018 at "Journal of separation science"
DOI: 10.1002/jssc.201800385
Abstract: A solid-phase microextraction probe was prepared on the surface of a stainless-steel wire through molecular sol-gel imprinting technology using chlorpyrifos as a template molecule, tetraethoxysilane as a sol-gel precursor, and acrylamide and β-cyclodextrin as functional… read more here.
Keywords: methyl; phase microextraction; preparation application; solid phase ... See more keywords
Application of solid-phase microextraction in current biomedical research.
Sign Up to like & getrecommendations! Published in 2019 at "Journal of separation science"
DOI: 10.1002/jssc.201800785
Abstract: Extraction of endogenous compounds and drugs and their corresponding metabolites from complex matrices, such as biofluids and solid tissues, requires adequate analytical approach facilitating qualitative and quantitative analysis. To this end, solid-phase microextraction has been… read more here.
Keywords: application solid; phase microextraction; solid phase; microextraction current ... See more keywords
Comparison of headspace solid-phase microextraction and solvent extraction method for simultaneous analysis of various soil fumigants in soil or water by gas chromatography-mass spectrometry.
Sign Up to like & getrecommendations! Published in 2020 at "Journal of separation science"
DOI: 10.1002/jssc.201900767
Abstract: The quantity of soil fumigants has increased globally which has focused attention on their environmental behavior. However, simultaneous analysis of traces of fumigant residues are often unreported because analysis methods are not readily available to… read more here.
Keywords: soil; headspace solid; phase microextraction; solid phase ... See more keywords
A rapid method for the quantification of urinary phthalate monoesters: a new strategy for the assessment of the exposure to phthalate ester by solid phase microextraction gas chromatography-tandem mass spectrometry.
Sign Up to like & getrecommendations! Published in 2020 at "Journal of separation science"
DOI: 10.1002/jssc.202000316
Abstract: In the following work, a new method for the analysis of the phthalate monoesters in human urine was reported. Phthalate monoesters are metabolites generated as a result of phthalate exposure. In compliance with the dictates… read more here.
Keywords: phthalate monoesters; phthalate; solid phase; phase microextraction ... See more keywords
Development of novel thin-film solid-phase microextraction materials based on deep eutectic solvents for preconcentration of trace amounts of parabens in surface waters.
Sign Up to like & getrecommendations! Published in 2022 at "Journal of separation science"
DOI: 10.1002/jssc.202100917
Abstract: A green and sensitive thin-film solid-phase microextraction method based on deep eutectic solvent was developed that enables simultaneous isolation, preconcentration, and determination of parabens in surface waters. Six new deep eutectic solvents were synthesized and… read more here.
Keywords: deep eutectic; phase microextraction; solid phase; film solid ... See more keywords