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Preparation and characterization of single crystals of tetrakis(4-(5,5-dimethyl-2-phenyl-1,3-dioxan-2-yl)phenyl)germane

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Published in 2019 at "Journal of Industrial and Engineering Chemistry"

DOI: 10.1016/j.jiec.2018.09.024

Abstract: Abstract A novel tetrakis(4-(5,5-dimethyl-2-phenyl-1,3-dioxan-2- yl)phenyl)germane (2) was synthesized by the reaction of germanium(IV) tetrachloride with 4-(5,5-dimethyl-2-phenyl-1,3-dioxan-2-yl)phenyllithium. Colorless plate-shaped single crystals obtained from recrystallization in ether were characterized by the single-crystal X-ray diffraction. The organogermanium compound… read more here.

Keywords: phenyl; dimethyl phenyl; tetrakis dimethyl; dioxan phenyl ... See more keywords