Selective One‐Pot Two‐Step C−C Bond Formation using Metal–Organic Frameworks with Mild Basicity as Heterogeneous Catalysts
Sign Up to like & getrecommendations! Published in 2017 at "ChemCatChem"
DOI: 10.1002/cctc.201700784
Abstract: Copper‐ion‐exchanged nickel pyrazolate frameworks behave as selective heterogeneous catalysts for the one‐pot, two‐step (Henry reaction/Michael type addition) synthesis of neuroactive pharmaceutical intermediates starting from nitromethane and benzaldehyde. Tuning the basicity of multifunctional metal–organic framework catalysts… read more here.
Keywords: pot two; heterogeneous catalysts; metal organic; two step ... See more keywords
One‐Pot Two‐Step Synthesis of Hydroxymethylated Unsaturated VHOSO and Its Application to the Synthesis of Biobased Polyurethanes
Sign Up to like & getrecommendations! Published in 2020 at "European Journal of Lipid Science and Technology"
DOI: 10.1002/ejlt.202000158
Abstract: In this study, we developed a one-pot two-step procedure to catalytically convert very high oleic sunflower oil (VHOSO) into hydroxymethylated unsaturated derivatives featuring both primary alcohols and carbon-carbon double bonds. The degree of functionalization in… read more here.
Keywords: two step; synthesis; pot two; one pot ... See more keywords
Facile synthesis of fused polyheterocycles containing trifluromethylated benzo[6,7]chromeno[2,3-c]pyrazoles via one-pot two-step MCRs
Sign Up to like & getrecommendations! Published in 2020 at "Journal of Fluorine Chemistry"
DOI: 10.1016/j.jfluchem.2020.109525
Abstract: Abstract A series of non-annulated products: trifluoromethylpyrazolone-tethered trisubstituted methane derivatives were synthesized in high yields in acetonitrile solvent catalyzed by NH4OAc via one-pot, three-component reactions of 2-hydroxy-1,4-naphthoquinone, aromatic aldehydes and 1-aryl-3-trifluoromethyl-5-pyrazolone. Treatment of trifluoromethylpyrazolone-tethered trisubstituted… read more here.
Keywords: benzo chromeno; pot two; two step; one pot ... See more keywords
Synthesis of benzocycloalkene derivatives via Pd-catalyzed one-pot two-step reactions of benzocyclic ketones, tosylhydrazide with aryl bromides
Sign Up to like & getrecommendations! Published in 2018 at "Journal of Saudi Chemical Society"
DOI: 10.1016/j.jscs.2018.02.003
Abstract: Abstract A new method for the synthesis of benzocycloalkene derivatives is described, through the palladium-catalyzed one-pot two-step reactions of benzocyclic ketones, tosylhydrazide with aryl bromides. Palladium-carbene complex as an important intermediate undergoes migratory insertion to… read more here.
Keywords: synthesis benzocycloalkene; benzocycloalkene derivatives; pot two; two step ... See more keywords
One-pot two-step stannylation/Stille homocoupling of aryl bromides and iodides under solvent-free conditions
Sign Up to like & getrecommendations! Published in 2018 at "Mendeleev Communications"
DOI: 10.1016/j.mencom.2018.05.032
Abstract: A new highly efficient solvent-free method for aryl bromide (iodide) homocoupling comprising the use of Pd(OAc)2/PCy3 system in the presence of CsF is suitable for substrates bearing functional groups not tolerant to lithium-, magnesium-, zincorganic… read more here.
Keywords: pot two; step stannylation; two step; one pot ... See more keywords
One-pot, two-step synthesis of 7-methylene-1,5-piperazine-fused 1,2,3-triazoles
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DOI: 10.1080/00397911.2020.1843178
Abstract: Abstract A facile, one-pot two-step synthesis of 7-methylene-1,5-piperazine-fused 1,2,3-triazole derivatives has been developed. The protocol employs an N-allylation of N-propargylated amines with 2,3-dibromopropene in the presence of K2CO3 in DMSO and a CuI-catalyzed [3 + 2] cycloaddition… read more here.
Keywords: pot two; two step; step synthesis; methylene ... See more keywords
A Rapid and Sensitive Detection of HIV-1 with a One-Pot Two-Stage Reverse Transcription Recombinase Aided Real-Time PCR Assay
Sign Up to like & getrecommendations! Published in 2023 at "Tropical Medicine and Infectious Disease"
DOI: 10.3390/tropicalmed8020105
Abstract: Human immunodeficiency virus 1 (HIV-1) attacks the immune system, making people susceptible to various diseases, thus increasing their risk of death. Comprehensive detection of major HIV-1 strains circulating in China is vital for effective HIV-1… read more here.
Keywords: time; pot two; hiv; two stage ... See more keywords