Triphenylphosphine Oxide Removal from Reactions: The Role of Solvent and Temperature
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DOI: 10.1021/acsomega.1c01996
Abstract: Here, a large-scale feasible, chromatography-free process to purge triphenylphosphine oxide (TPPO) from the crude product of Mitsunobu and Wittig reactions has been developed. Divergence in physicochemical properties like polarity and solubility of TPPO against the… read more here.
Keywords: triphenylphosphine oxide; removal reactions; role solvent; oxide removal ... See more keywords