One-Pot Sequential Hydrogen Isotope Exchange/Reductive Deuteration for the Preparation of α,β-Deuterated Alcohols using Deuterium Oxide.
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DOI: 10.1021/acs.orglett.2c01940
Abstract: An efficient one-pot sequential hydrogen isotope exchange (HIE)/reductive deuteration approach was developed for the preparation of α,β-deuterated alcohols using ketones as the precursors. The HIE step can also be used for the synthesis of α-deuterated… read more here.
Keywords: sequential hydrogen; isotope exchange; one pot; reductive deuteration ... See more keywords