Determination of the 15N chemical shift anisotropy in natural abundance samples by proton‐detected 3D solid‐state NMR under ultrafast MAS of 70 kHz
Sign Up to like & getrecommendations! Published in 2019 at "Magnetic Resonance in Chemistry"
DOI: 10.1002/mrc.4841
Abstract: Chemical shift anisotropy (CSA) is a sensitive probe of electronic environment at a nucleus, and thus, it offers deeper insights into detailed structural and dynamic properties of different systems, for example, chemical, biological, and materials.… read more here.
Keywords: khz; chemical shift; ultrafast mas; 15n csa ... See more keywords
Rapid automated determination of chemical shift anisotropy values in the carbonyl and carboxyl groups of fd-y21m bacteriophage using solid state NMR
Sign Up to like & getrecommendations! Published in 2018 at "Journal of Biomolecular NMR"
DOI: 10.1007/s10858-018-0206-1
Abstract: Determination of chemical shift anisotropy (CSA) in immobilized proteins and protein assemblies is one of several tools to determine protein dynamics on the timescales of microseconds and faster. The large CSA values of C=O groups… read more here.
Keywords: shift anisotropy; determination chemical; csa; chemical shift ... See more keywords
Measurement of amide proton chemical shift anisotropy in perdeuterated proteins using CSA amplification.
Sign Up to like & getrecommendations! Published in 2017 at "Journal of magnetic resonance"
DOI: 10.1016/j.jmr.2017.09.009
Abstract: Measuring 1H chemical shift anisotropy (CSA) is useful for probing proton environments and dynamics but remains a challenge due to strong homonuclear interaction and relatively small shift anisotropy, especially in proteins with multiple proton sites.… read more here.
Keywords: shift; chemical shift; amide proton; shift anisotropy ... See more keywords