Electrochemical sulfonylation of thiols with sulfonyl hydrazides: a metal- and oxidant-free protocol for the synthesis of thiosulfonates
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DOI: 10.1039/c8gc02143k
Abstract: An efficient electrochemical transformation of structurally diverse sulfonyl hydrazides and thiols into thiosulfonates in the presence of ammonium iodide as redox catalyst and electrolyte in acetonitrile at ambient temperature is reported. Transition metal- and oxidant-free… read more here.
Keywords: electrochemical sulfonylation; sulfonylation thiols; metal oxidant; sulfonyl hydrazides ... See more keywords