Articles with "synthesis characterisation" as a keyword



Sulfonated N-heterocyclic carbine-silver (I) complexes: Synthesis, characterisation and biological evaluation

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Published in 2018 at "Applied Organometallic Chemistry"

DOI: 10.1002/aoc.4016

Abstract: The synthesis, characterisation and biological activity of water-soluble Ag(I)-NHC complexes, general formula Na[(NHC)AgCl] where NHC is a sulfonated and sterically hindered N-heterocyclic carbene, is reported. The Ag-NHC complexes (2a–e) were synthesised by reacting the corresponding… read more here.

Keywords: heterocyclic carbine; characterisation biological; sulfonated heterocyclic; synthesis characterisation ... See more keywords

Synthesis, Characterisation, Magnetic Properties, and DFT Investigations of Heterobimetallic Nickel‐Lanthanide LNiIILnIII(Ln = Ce, Gd, Tb, Dy) Complexes Supported by Schiff Base Ligands

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Published in 2025 at "European Journal of Inorganic Chemistry"

DOI: 10.1002/ejic.202500229

Abstract: Four heterobimetallic complexes (Ln = Ce (2), Gd (3), Tb (4), and Dy (5), H2L= Schiff base ligand) were synthesized from LNi (1) precursor (H2L = ligand N, N’‐bis(3‐methoxysalicylaldiimine)‐1,3‐propylene‐2‐ol). Compound 2, which crystallizes in the… read more here.

Keywords: characterisation magnetic; synthesis characterisation; schiff base; magnetic properties ... See more keywords

Synthesis and characterisation of Al4O4C nanorod/CNT composites

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Published in 2017 at "Ceramics International"

DOI: 10.1016/j.ceramint.2017.05.352

Abstract: Abstract A novel route has been developed to synthesise Al 4 O 4 C nanorod/CNT composites by heat-treating Al 4 SiC 4 in a furnace with carbon heater. The study of growth mechanism indicates that… read more here.

Keywords: synthesis characterisation; cnt composites; nanorod cnt; characterisation al4o4c ... See more keywords

Copper doped nickel aluminate: Synthesis, characterisation, optical and colour properties

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Published in 2019 at "Chinese Journal of Chemical Engineering"

DOI: 10.1016/j.cjche.2019.01.008

Abstract: Abstract Novel environment friendly inorganic nano green pigments, Ni1−xCuxAl2O4 (x = 0, 0.02, 0.04, 0.06, 0.08, 0.1) were successfully synthesised by simple, cost effective sol–gel method using citric acid as a gelling agent. Synthesised nano pigments were… read more here.

Keywords: aluminate synthesis; synthesis characterisation; nickel aluminate; copper doped ... See more keywords
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Synthesis, characterisation and protonation of phosphate disubstituted derivatives with pyridyl-functionalized diiron

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Published in 2018 at "Inorganica Chimica Acta"

DOI: 10.1016/j.ica.2017.11.028

Abstract: Abstract Three new phosphine disubstituted derivatives of [2Fe2S] model complexes with pendant pyridine family, [(μ-SEt)(μ-SCH2C6H4N)Fe2(CO)4(L)2] (2, L = PPh3; 3, L = dppm; 4, L = PMe3), have been synthesized and the molecular structure of 2 was determinated by single crystal… read more here.

Keywords: synthesis characterisation; disubstituted derivatives; characterisation protonation; protonation ... See more keywords

Synthesis and characterisation of platinum(IV) polypyridyl complexes with halide axial ligands

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Published in 2019 at "Inorganica Chimica Acta"

DOI: 10.1016/j.ica.2019.118964

Abstract: Abstract A series of complexes of the type [Pt(PL)(AL)(X)2]2+ (where PL = 1,10-phenanthroline, 5-methyl-1,10-phenanthroline or 5,6-dimethyl-1,10-phenanthroline; AL = 1S,2S-diaminocyclohexane and, X = Cl, Br or I) with anticancer potency, were synthesised in a one pot reaction using N-halogensuccinimide (NXS) as both… read more here.

Keywords: polypyridyl complexes; synthesis characterisation; platinum polypyridyl; axial ligands ... See more keywords

Synthesis and characterisation of chitin from periwinkle (Tympanotonus fusatus (L.)) and snail (Lissachatina fulica (Bowdich)) shells.

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Published in 2018 at "International journal of biological macromolecules"

DOI: 10.1016/j.ijbiomac.2017.08.106

Abstract: This study characterizes chitin extracted from bio-sources of snail and periwinkle using varied combinations of acid and alkali concentrations. A three level factorial design of experiment with alkali and acid concentrations was used. FTIR, XRD… read more here.

Keywords: chitin periwinkle; synthesis characterisation; periwinkle; chitin ... See more keywords

Synthesis and characterisation of robust emulsion-templated silica microcapsules.

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Published in 2017 at "Journal of colloid and interface science"

DOI: 10.1016/j.jcis.2017.06.026

Abstract: Robust silica microcapsules were synthesised using an emulsion template via a seeded growth strategy. Multiple additions of the silica precursor tetraethyl orthosilicate (TEOS) were observed to result in a number of physical and property changes… read more here.

Keywords: synthesis characterisation; robust emulsion; silica microcapsules; synthesis ... See more keywords

Synthesis and characterisation of the hollandite solid solution Ba1.2-xCsxFe2.4-xTi5.6+xO16 for partitioning and conditioning of radiocaesium

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Published in 2018 at "Journal of Nuclear Materials"

DOI: 10.1016/j.jnucmat.2018.03.005

Abstract: Abstract The geological disposal of high level radioactive waste requires careful budgeting of the heat load produced by radiogenic decay. Removal of high-heat generating radionuclides, such as 137Cs, reduces the heat load in the repository… read more here.

Keywords: synthesis characterisation; solution ba1; solution; solid solution ... See more keywords

Ionothermal synthesis and characterisation of Mn-, Co-, Fe- and Ni-containing aluminophosphates

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Published in 2018 at "Microporous and Mesoporous Materials"

DOI: 10.1016/j.micromeso.2018.06.045

Abstract: Abstract Metalloaluminophosphates (MAPOs) containing different metal ions (Mn3+, Mn2+, Co2+, Fe2+ or Ni2+) were synthesised in ionic liquids to investigate the effect of changing ionic liquid structure, reaction time, the nature of metal ions, and… read more here.

Keywords: synthesis characterisation; framework; metal; characterisation containing ... See more keywords

Synthesis, characterisation and antioxidant properties of ferulate-based protic ionic liquids: Experimental and modelling approaches

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Published in 2019 at "Journal of Molecular Liquids"

DOI: 10.1016/j.molliq.2019.01.048

Abstract: Abstract Active pharmaceutical ingredients (APIs) in the form of crystalline solid are commonly produced in drug manufacturing industries. However, crystalline solid APIs have a low solubility and the ability to cause polymorphism transformation. In order… read more here.

Keywords: protic ionic; ferulate based; synthesis characterisation; antioxidant activity ... See more keywords